2-Nitro-N-(8-quinolyl)benzamide
نویسندگان
چکیده
In the title compound, C(16)H(11)N(3)O(3), the amide group is twisted away from the quinoline ring system and nitro-benzene ring by 8.02 (1)° and 54.92 (1)°, respectively. The crystal packing is stabilized by inter-molecular C-H⋯O hydrogen bonds, and π-π inter-actions between the quinoline ring systems of inversion-related mol-ecules, with a centroid-centroid distance of 3.4802 (13) Å.
منابع مشابه
Synthesis, Characterization and Anti-Inflammatory Activity of Some 1, 3,4 -Oxadiazole Derivatives
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In the title compound, C(16)H(11)N(3)O(3), the amide group is twisted away from the plane of the quinoline benzene ring by 3.93 (5)°, but is twisted away from the nitro-benzene ring by 22.68 (4)°. A weak intra-molecular C-H⋯O hydrogen bond is observed. In the crystal structure, mol-ecules are linked into a chain along the a axis by inter-molecular C-H⋯O hydrogen bonds.
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A series of five-membered heterocyclic rings were synthesized by the reaction between benzoyl chloride and various chlolro-nitro-benzoyl chlorides and semi carbazide to form (C1-C7) compounds and was tested for their anti-inflammatory activity determined by rat-paw-oedema method. All the synthesis compounds have been characterized by 1HNMR, IR and Mass spectral data. The compounds were purified...
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